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Chemical Effect Analyses of 3d Elements by Study of X-Ray Fluorescence SpectraDurdaği, Sevil(Porikli)Asymmetry indexChemical effectRelative intensity ratioWavelength dispersive X-ray spectroscopy (WDXRF)Rhodium metallographySingle crystalsSpectrometersSulfur compoundsTransition metal compoundsTransition metalsX ray spectroscopyX ray tubes3d transition metalsEnergy shiftLorentz functionsRelative intensityWavelength dispersive X-ray spectroscopiesX ray fluorescenceChemical analysisSpectra of K X-rays emitted from pure 3d transition metals and their oxide and sulfate compounds were measured using a single crystal wavelength dispersive X-ray spectroscopy (WDXRF). The measurements were performed using a ZSX-100e sequential spectrometer equipped with an Rh X-ray tube operated. An accurate analytical representation of each line was obtained by a fit to a Lorentz function. The spectra were analyzed in order to examine the K X-ray peak parameters such as asymmetry index, peak energy and relative intensity ratios. The energy shifts and relative intensities weredetermined tobetter understand the chemical effect. © 2018, Peking University Press. All right reserved.Science Press2018Articlehttps://rdlopen.rawdatalibrary.net/r/ebyu/14174https://doi.org/10.3964/j.issn.1000-0593(2018)08-2630-081000-0593enGuang Pu Xue Yu Guang Pu Fen Xi/Spectroscopy and Spectral Analysisinfo:eu-repo/semantics/openAccessinfo:eu-repo/semantics/articlehttps://ebyu-rdlopen.rawdatalibrary.net/tr/items/ebyu/14174